Thionyl Chloride → HCID 19972568, compound

HRID 1580301Notes

Reaction equation

HRID 1580301 reaction equation
O[CH2:2][CH2:3][O:4][C:5]1[CH:10]=[CH:9][CH:8]=[CH:7][C:6]=1[S:11][CH3:12].S(Cl)([Cl:15])=O>>[Cl:15][CH2:2][CH2:3][O:4][C:5]1[CH:10]=[CH:9][CH:8]=[CH:7][C:6]=1[S:11][CH3:12]

Participants

3

Reactant 2

HCID 24386Thionyl ChlorideHCID 22036270o-(beta-Hydroxyethoxy)-thioanisole

Product 1

HCID 19972568HCID 19972568, compound

Procedure

o-(β-Hydroxyethoxy)-thioanisole (0.1 mole) is refluxed in excess thionyl chloride and evaporated to dryness to yield o-(β-chloroethoxy)-thioanisole.

Workup

  1. customevaporated to dryness

Sources & evidence

ORD record
ord-43f3c1c561d040579f5f65e63a4f5f8f
Source dataset
uspto-grants-1976_01
Patent number
US03932498

Reaction notes

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