HuagongsheHuagongshe Chemistry Print Report · For research reference only
Z-Ala-Ile-Gly-OMe → H-Ala-Ile-Gly-OMe
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Z-Ala-Ile-Gly-OMe | HCID 131709979 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | H-Ala-Ile-Gly-OMe | HCID 131709978 | — |
Reaction Steps
2.0 g of Z-Ala-Ile-Gly-OMe are dissolved in 40 ml of methanol with gentle warming and then hydrogenated in the presence of 300 mg of Pd on charcoal (10 %). After completion of the hydrogenation the catalyst is filtered off and the filtrate completely evaporated to dryness. The residue, which is homogeneous in a thin layer chromatogram, is immediately processed further.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03934008 |
| Source dataset | uspto-grants-1976_01 |
| ORD ID | ord-018578aaaca64d8a879870cebd4941a8 |
| Source note | uspto-grants-1976_01 |