HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Methoxy-5-nitroaniline → HCID 21560402, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Methoxy-5-nitroaniline | HCID 7447 | — |
| Reactant | 2-Chloro-5-nitroaniline | HCID 22691 | — |
| Reactant | (2,4,6-Trichlorophenyl)hydrazine | HCID 79234 | — |
| Reactant | 2-Propenoic acid, 3,3-diethoxy-, ethyl ester | HCID 169388 | — |
| Product | HCID 21560402 | HCID 21560402 | — |
Reaction Steps
Using the same procedure as Method (a) in Synthesis Example 1, in place of 2-chloro-5-nitroaniline, 2-methoxy-5-nitroaniline was reacted with β,β-diethoxyacrylic acid ethyl ester and then the reaction product was further reacted with 2,4,6-trichloro phenylhydrazine to give the desired product having a melting point of 254°C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03935015 |
| Source dataset | uspto-grants-1976_01 |
| ORD ID | ord-3aef10c45d4d42bea70f6fdf6a07af18 |
| Source note | uspto-grants-1976_01 |