Myristoyl chloride → HCID 21560402, compound

HRID 1580913Notes

Reaction equation

HRID 1580913 reaction equation
[Cl:1][C:2]1[CH:7]=[C:6]([Cl:8])[CH:5]=[C:4]([Cl:9])[C:3]=1[N:10]1[C:14](=[O:15])[CH:13]=[C:12]([NH:16][C:17]2[CH:22]=[C:21]([NH2:23])[CH:20]=[CH:19][C:18]=2[O:24][CH3:25])[NH:11]1.[C:26](Cl)(=[O:40])[CH2:27][CH2:28][CH2:29][CH2:30][CH2:31][CH2:32][CH2:33][CH2:34][CH2:35][CH2:36][CH2:37][CH2:38][CH3:39]>>[Cl:1][C:2]1[CH:7]=[C:6]([Cl:8])[CH:5]=[C:4]([Cl:9])[C:3]=1[N:10]1[C:14](=[O:15])[CH:13]=[C:12]([NH:16][C:17]2[CH:22]=[C:21]([NH:23][C:26](=[O:40])[CH2:27][CH2:28][CH2:29][CH2:30][CH2:31][CH2:32][CH2:33][CH2:34][CH2:35][CH2:36][CH2:37][CH2:38][CH3:39])[CH:20]=[CH:19][C:18]=2[O:24][CH3:25])[NH:11]1

Participants

3

Reactant 2

HCID 66986Myristoyl chlorideHCID 21560403HCID 21560403, compound

Product 1

HCID 21560402HCID 21560402, compound

Procedure

The 1-(2,4,6-trichlorophenyl)-3-(2-methoxy-5-aminoanilino)-5-pyrazolone prepared in the above procedure was reacted with myristic acid chloride prepared using Method (3) of Synthesis Example 1 to give the desired product having a melting point of 89°-93°C.

Workup

  1. customprepared
  2. customMethod (3) of Synthesis Example 1

Sources & evidence

ORD record
ord-a6235fd7ed0b4b60b6ad6d072a2fa9d9
Source dataset
uspto-grants-1976_01
Patent number
US03935015

Reaction notes

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