Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Diisobutylamine | HCID 8085 | — |
| Reactant | Butyllithium | HCID 178418339 | — |
| Solvent | Hexane | HCID 8058 | — |
| Product | Lithium diisobutylamide | HCID 11018925 | — |
Reaction Steps
4 ml n-butyl-lithium solution and 1.38 ml di-i-butylamine are added to 1 l n-hexane and the mixture is stirred for 15 minutes at 20°C with exclusion of air and moisture. A solution of lithium di-i-butylamide is obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US03935177 |
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| Source dataset | uspto-grants-1976_01 |
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| ORD ID | ord-00acaa52d6ff4177b092aff365baddc3 |
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| Source note | uspto-grants-1976_01 |
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