HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-(Chloromethyl)-1-methoxy-4-nitrobenzene → N-methyl-N-(5-nitro-2-methoxybenzyl)N,N-bis(3-formamidopropyl)ammonium chloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-(Chloromethyl)-1-methoxy-4-nitrobenzene | HCID 2529377 | — |
| Reactant | Formamide, N,N'-[(methylimino)di-3,1-propanediyl]bis- | HCID 3084810 | — |
| Solvent | Water | HCID 962 | — |
| Product | N-methyl-N-(5-nitro-2-methoxybenzyl)N,N-bis(3-formamidopropyl)ammonium chloride | HCID 20336842 | — |
Reaction Steps
Proceeding in a manner similar to that described above in B-8a, 142 parts of N,N-bis(3-formamidopropyl)methylamine and 141 parts of 5-nitro-2-methoxybenzyl chloride were interacted in 115 parts of water to obtain N-methyl-N-(5-nitro-2-methoxybenzyl)-N,N-bis(3-formamidopropyl)ammonium chloride. The product was not isolated but was used directly in solution for reduction of the nitro group.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03935182 |
| Source dataset | uspto-grants-1976_01 |
| ORD ID | ord-6925b875a4cf4b428ed118ace7789f52 |
| Source note | uspto-grants-1976_01 |