Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
N-(3-(dimethylamino)propyl)formamide → N,N-dimethyl-N-(5-nitro-2-methoxyphenyl)carbamylmethyl-N-3-formamidopropylammonium chloride
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | N-(3-(dimethylamino)propyl)formamide | HCID 80020 | — |
| 반응물 | 2-chloro-N-(2-methoxy-5-nitrophenyl)acetamide | HCID 2362603 | — |
| 용매 | Isopropanol | HCID 3776 | — |
| 생성물 | N,N-dimethyl-N-(5-nitro-2-methoxyphenyl)carbamylmethyl-N-3-formamidopropylammonium chloride | HCID 86733013 | — |
반응 단계
In a manner similar to that described above in B-1a, and using 27.3 parts of N-(3-dimethylaminopropyl)formamide, 48 parts of 2-chloro-2'-methoxy-5'-nitroacetanilide, and 157 parts of isopropyl alcohol there was obtained 52.6 parts of N,N-dimethyl-N-(5-nitro-2-methoxyphenyl)carbamylmethyl-N-3-formamidopropylammonium chloride as a white solid, m.p. 86°-88°C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US03935182 |
| 출처 데이터셋 | uspto-grants-1976_01 |
| ORD ID | ord-d2b9cc6f616b45a6bcddbff9411e7041 |
| 출처 메모 | uspto-grants-1976_01 |