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HRID1580940

反应详情

EQUATION

反应方程式

HRID 1580940 的结构方程式

REACTANTS

反应物

3
结构：COc1cc(C(C)=O)cc(OC)c1OC
HCID14345

3',4',5'-Trimethoxyacetophenone

C11H14O4

结构：C[O-].[Na+]
HCID10942334

Methanol, sodium salt

CH3NaO

结构：Cc1nc2c(C)cccn2c(=O)c1C
HCID12339719

2,3,9-Trimethyl-4H-pyrido[1,2-a]pyrimidin-4-one

C11H12N2O

PRODUCTS

生成物

1
结构：COc1cc(C(C)=Cc2nc3c(C)cccn3c(=O)c2C)cc(OC)c1OC
HCID56638083

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CO
溶剂HCID887

Methanol

CH4O

PROCEDURE

实验过程

To a solution of 1.3g of sodium methoxide in 75 ml of absolute methanol is added 2.0g of 2,3,9-trimethyl-4H-pyrido[1,2-a]pyrimidin-4-one, followed by 4.2g of 3,4,5-trimethoxyacetophenone. The mixture is stirred and heated under reflux for 97 hours to yield the title compound.

WORKUP

后处理

  1. temperatureheated
  2. temperatureunder reflux for 97 hours