2-Chloro-N,N-dimethylethylamine → HCID 86733023, compound

HRID 1581008Notes

Reaction equation

HRID 1581008 reaction equation
[Cl:1][C:2]1[CH:3]=[C:4]([CH:18]=[CH:19][C:20]=1[Cl:21])[CH2:5][N:6]1[CH2:11][CH2:10][NH:9][CH2:8][CH:7]1[C:12]1[CH:17]=[CH:16][CH:15]=[CH:14][CH:13]=1.[CH2:22]([N:24]([CH2:27]CCl)[CH2:25]C)[CH3:23].CN(CCCl)C>>[Cl:1][C:2]1[CH:3]=[C:4]([CH:18]=[CH:19][C:20]=1[Cl:21])[CH2:5][N:6]1[CH2:11][CH2:10][N:9]([CH2:23][CH2:22][N:24]([CH3:27])[CH3:25])[CH2:8][CH:7]1[C:12]1[CH:17]=[CH:16][CH:15]=[CH:14][CH:13]=1

Participants

4

Reactant 3

HCID 79012-Chloro-N,N-dimethylethylamineHCID 13364Diethylaminoethyl chlorideHCID 21448557HCID 21448557, compound

Product 1

HCID 86733023HCID 86733023, compound

Procedure

1-(3',4'-Dichloro benzyl)-2-phenyl piperazine prepared according to Example 3b, is alkylated by following the procedure described in Example 3c, whereby, in place of diethylamino ethylchloride, the equimolecular amount of dimethylamino ethylchloride is used. The resulting reaction product is obtained in the form of a light yellow oil boiling at 190° C./0.01 mm. Hg.

Workup

  1. customThe resulting reaction product

Sources & evidence

ORD record
ord-98803735f1ba4d9588ddae6caefc9f47
Source dataset
uspto-grants-1976_01
Patent number
US03935214

Reaction notes

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