Diethylaminoethyl chloride → HCID 54042764, compound

HRID 1581010Notes

Reaction equation

HRID 1581010 reaction equation
[Cl:1][C:2]1[CH:3]=[C:4]([CH:18]=[CH:19][C:20]=1[Cl:21])[CH2:5][N:6]1[CH2:11][CH2:10][NH:9][CH2:8][CH:7]1[C:12]1[CH:17]=[CH:16][CH:15]=[CH:14][CH:13]=1.C(N(CCCl)CC)C.[CH2:30]([N:32]([CH2:35][CH2:36][CH2:37]Cl)[CH2:33][CH3:34])[CH3:31]>>[Cl:1][C:2]1[CH:3]=[C:4]([CH:18]=[CH:19][C:20]=1[Cl:21])[CH2:5][N:6]1[CH2:11][CH2:10][N:9]([CH2:37][CH2:36][CH2:35][N:32]([CH2:33][CH3:34])[CH2:30][CH3:31])[CH2:8][CH:7]1[C:12]1[CH:17]=[CH:16][CH:15]=[CH:14][CH:13]=1

Participants

4

Reactant 3

HCID 13364Diethylaminoethyl chlorideHCID 669183-Chloropropyl(diethyl)amineHCID 21448557HCID 21448557, compound

Product 1

HCID 54042764HCID 54042764, compound

Procedure

1-(3',4'-Dichloro benzyl)-2-phenyl piperazine prepared according to Example 3b, is alkylated by following the procedure described in Example 3c whereby, in place of diethylamino ethylchloride, the equimolecular amount of diethylamino propylchloride is used. The resulting reaction product is obtained in the form of a light yellow oil boiling at 210° C./0.04 mm. Hg.

Workup

  1. customThe resulting reaction product

Sources & evidence

ORD record
ord-fd0acafb9a74483da0a62fdd491495c0
Source dataset
uspto-grants-1976_01
Patent number
US03935214

Reaction notes

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