Diethylaminoethyl chloride → HCID 54566101, compound
Reaction equation
[CH2:1]([O:8][C:9]1[CH:27]=[CH:26][C:12]([CH2:13][N:14]2[CH2:19][CH2:18][NH:17][CH2:16][CH:15]2[C:20]2[CH:25]=[CH:24][CH:23]=[CH:22][CH:21]=2)=[CH:11][CH:10]=1)[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.[CH2:28]([N:30]([CH2:33][CH2:34]Cl)[CH2:31][CH3:32])[CH3:29]>>[CH2:1]([O:8][C:9]1[CH:27]=[CH:26][C:12]([CH2:13][N:14]2[CH2:19][CH2:18][N:17]([CH2:29][CH2:28][N:30]([CH2:33][CH3:34])[CH2:31][CH3:32])[CH2:16][CH:15]2[C:20]2[CH:21]=[CH:22][CH:23]=[CH:24][CH:25]=2)=[CH:11][CH:10]=1)[C:2]1[CH:3]=[CH:4][CH:5]=[CH:6][CH:7]=1Participants
3
Procedure
1-(4'-Benzyloxy benzyl)-2-phenyl piperazine prepared according to Example 16, is alkylated by means of diethylamino ethylchloride by following the procedure described in Example 3c. The resulting reaction product is obtained in the form of a light yellow oil boiling at 235° C./0.01 mm. Hg.
Workup
- customThe resulting reaction product
Sources & evidence
- ORD record
- ord-32d1ed91daab410e8914c8c340d39787
- Source dataset
- uspto-grants-1976_01
- Patent number
- US03935214
Reaction notes
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