Morpholine → HCID 10193835, compound

HRID 1581469Notes

Reaction equation

HRID 1581469 reaction equation
[NH:1]1[CH2:6][CH2:5][O:4][CH2:3][CH2:2]1.C([O:14][C:15](=O)[NH:16][C:17]1[S:21][C:20]2[C:22]([C:28]3[CH:33]=[CH:32][CH:31]=[CH:30][CH:29]=3)=[CH:23][CH:24]=[C:25]([O:26][CH3:27])[C:19]=2[CH:18]=1)C1C=CC=CC=1>>[CH3:27][O:26][C:25]1[C:19]2[CH:18]=[C:17]([NH:16][C:15]([N:1]3[CH2:6][CH2:5][O:4][CH2:3][CH2:2]3)=[O:14])[S:21][C:20]=2[C:22]([C:28]2[CH:33]=[CH:32][CH:31]=[CH:30][CH:29]=2)=[CH:23][CH:24]=1

Participants

3

Reactant 2

HCID 8083MorpholineHCID 20724759HCID 20724759, compound

Product 1

HCID 10193835HCID 10193835, compound

Procedure

The title compound MS: mi/e=369.3 (M+H+) was obtained as a light brown solid (58% yield) by the reaction of morpholine with (4-methoxy-7-phenyl-benzo[b]thiophen-2-yl)-carbamic acid benzyl ester according to the method described above for example 1.

Sources & evidence

ORD record
ord-ddd4b39944744820839c576830ec4cf5
Source dataset
uspto-grants-2004_05
Patent number
US06730670B2

Reaction notes

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