Bromine → HCID 19007564, compound

HRID 1581478Notes

Reaction equation

HRID 1581478 reaction equation
[CH3:1][O:2][C:3]([C:5]1[S:9][C:8]2[CH:10]=[CH:11][CH:12]=[C:13]([O:14][CH3:15])[C:7]=2[CH:6]=1)=[O:4].[Br:16]Br>C(Cl)(Cl)Cl>[CH3:1][O:2][C:3]([C:5]1[S:9][C:8]2[C:10]([Br:16])=[CH:11][CH:12]=[C:13]([O:14][CH3:15])[C:7]=2[CH:6]=1)=[O:4]

Participants

4

Reactant 2

HCID 24408BromineHCID 17750023Methyl 4-methoxy-1-benzothiophene-2-carboxylate

Product 1

HCID 19007564HCID 19007564, compound

Reagents, catalysts & solvents 1

HCID 6212ChloroformSolvent

Procedure

The title compound was prepared as an off-white solid (m.p. 112° C.) according to the literature by treatment of 4-methoxy-benzo[b]thiophene-2-carboxylic acid methyl ester with bromine in chloroform at 0° C. to 20° C.

Sources & evidence

ORD record
ord-4ec40654f8d64bfc8bd2b30c4186b3ac
Source dataset
uspto-grants-2004_05
Patent number
US06730670B2

Reaction notes

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