HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Nitrobenzenesulfonyl chloride → HCID 53708043, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Nitrobenzenesulfonyl chloride | HCID 15540 | — |
| Reactant | HCID 54000894 | HCID 54000894 | — |
| Product | HCID 53708043 | HCID 53708043 | 40.9% |
Reaction Steps
Using the general procedure described in step A of scheme 1, (6-amino-6-cyano-hexyl}-carbamic acid benzyl ester (2.8 g, 10 mmol) was sulfonylated with 2-nitrobenzenesulfonyl chloride (2.5 g, 11 mmol) at 0° C. to yield the titled compound (1.7 g, 36%); yellow oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06734182B2 |
| Source dataset | uspto-grants-2004_05 |
| ORD ID | ord-58dba28be26c4fb495e991ae69e2d738 |
| Source note | uspto-grants-2004_05 |