HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl morpholine oxide → 1-(1-Ethyl-6-isopropyl-4,4-dimethyl-1,2,3,4-tetrahydro-quinolin-8-yl)-propan-1-one
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl morpholine oxide | HCID 82029 | — |
| Reactant | 1-(1-Ethyl-6-isopropyl-4,4-dimethyl-1,2,3,4-tetrahydro-quinolin-8-yl)-propan-1-ol | HCID 22719819 | — |
| Product | 1-(1-Ethyl-6-isopropyl-4,4-dimethyl-1,2,3,4-tetrahydro-quinolin-8-yl)-propan-1-one | HCID 22719825 | — |
Reaction Steps
Following General Procedure D, 1-(1-ethyl-6-isopropyl-4,4-dimethyl-1,2,3,4-tetrahydro-quinolin-8-yl)-propan-1-ol (Intermediate 10, 5.37 g, 21.3 mmol) and 4-methylmorpholine N-oxide (5.00 g, 42.6 mmol) were reacted to give the title compound as a yellow oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06734193B1 |
| Source dataset | uspto-grants-2004_05 |
| ORD ID | ord-ac062a2474f643c2813a73043fb6f2f9 |
| Source note | uspto-grants-2004_05 |