HuagongsheHuagongshe Chemistry Print Report · For research reference only
Azobisisobutyronitrile → HCID 86587240, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Azobisisobutyronitrile | HCID 6547 | — |
| Reactant | N-Methylmaleimide | HCID 70261 | — |
| Reactant | HCID 86587194 | HCID 86587194 | — |
| Reactant | HCID 86587195 | HCID 86587195 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 86587240 | HCID 86587240 | — |
Reaction Steps
To 20 mL of tetrahydrofuran was added 10 mmole of N-methylmaleimide, 10 mmole of hexafluorobutyl-5-norbornene-2-carboxylate, 80 mmole of 2,6-difluoro-1-methylbenzylacrylate and 0.3 9 of AIBN, and the resulting solution was reacted at about 65° C. for about 12 hours.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06737217B2 |
| Source dataset | uspto-grants-2004_05 |
| ORD ID | ord-b23219e41b814d6486b6d04466eaca3c |
| Source note | uspto-grants-2004_05 |