1-Tridecanol → 1-Dodecene

HRID 1582792Notes

Reaction equation

[CH2:1](O)[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12]C.[BH4-].[Na+]>>[CH2:1]=[CH:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH3:12]

Participants

Reactant 2

HCID 82071-Tridecanol

HCID 4311764Sodium borohydride

Product 1

HCID 81831-Dodecene

Procedure

450 g of a tridecanol fraction prepared in this manner are post-hydrogenated with 3.5 g of NaBH4.

Sources & evidence

ORD record: ord-ae9a2972b0204e34848efb7610aaa440
Source dataset: uspto-grants-2004_05
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US06737553B1

Reaction notes

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