4-Nitrobenzoyl chloride → HCID 86759451, compound

HRID 1582852Notes

Reaction equation

HRID 1582852 reaction equation
[CH2:1]([O:7][C:8](=[O:17])[C:9]1[CH:14]=[C:13]([NH2:15])[CH:12]=[C:11]([NH2:16])[CH:10]=1)[CH2:2][CH2:3][CH2:4][CH2:5][CH3:6].[N+:18]([C:21]1[CH:29]=[CH:28][C:24]([C:25](Cl)=[O:26])=[CH:23][CH:22]=1)([O-:20])=[O:19]>>[CH2:1]([O:7][C:8](=[O:17])[C:9]1[CH:10]=[C:11]([NH:16][C:25](=[O:26])[C:24]2[CH:28]=[CH:29][C:21]([N+:18]([O-:20])=[O:19])=[CH:22][CH:23]=2)[CH:12]=[C:13]([NH:15][C:25](=[O:26])[C:24]2[CH:23]=[CH:22][C:21]([N+:18]([O-:20])=[O:19])=[CH:29][CH:28]=2)[CH:14]=1)[CH2:2][CH2:3][CH2:4][CH2:5][CH3:6]

Participants

3

Reactant 2

HCID 85024-Nitrobenzoyl chlorideHCID 22501534HCID 22501534, compound

Product 1

HCID 86759451HCID 86759451, compoundYield 82%

Procedure

Using n-hexyl-3,5-diaminobenzoate (24.0 g, 101.7 mmol) and 4-nitrobenzoyl chloride (39.7 g, 214.4 mmol), n-hexyl[3,5-bis(4-nitrobenzoylamino)]benzoate was obtained (44.5 g, yield: 82%) in the same manner as in Example 1.

Sources & evidence

ORD record
ord-6756946c8c50447983483e4dbd20c1cf
Source dataset
uspto-grants-2004_05
Patent number
US06740371B1

Reaction notes

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