Cetyl Alcohol → HCID 86759452, compound

HRID 1582854Notes

Reaction equation

[N+:1]([C:4]1[CH:29]=[CH:28][C:7]([O:8][C:9]2[CH:10]=[C:11]([CH:15]=[C:16]([O:18][C:19]3[CH:24]=[CH:23][C:22]([N+:25]([O-:27])=[O:26])=[CH:21][CH:20]=3)[CH:17]=2)[C:12]([O-:14])=[O:13])=[CH:6][CH:5]=1)([O-:3])=[O:2].[CH2:30](O)[CH2:31][CH2:32][CH2:33][CH2:34][CH2:35][CH2:36][CH2:37][CH2:38][CH2:39][CH2:40][CH2:41][CH2:42][CH2:43][CH2:44][CH3:45]>>[CH2:45]([O:13][C:12](=[O:14])[C:11]1[CH:10]=[C:9]([O:8][C:7]2[CH:6]=[CH:5][C:4]([N+:1]([O-:3])=[O:2])=[CH:29][CH:28]=2)[CH:17]=[C:16]([O:18][C:19]2[CH:24]=[CH:23][C:22]([N+:25]([O-:27])=[O:26])=[CH:21][CH:20]=2)[CH:15]=1)[CH2:44][CH2:43][CH2:42][CH2:41][CH2:40][CH2:39][CH2:38][CH2:37][CH2:36][CH2:35][CH2:34][CH2:33][CH2:32][CH2:31][CH3:30]

Participants

Reactant 2

HCID 2682Cetyl Alcohol

HCID 22715474HCID 22715474, compound

Product 1

HCID 86759452HCID 86759452, compoundYield 81%

Procedure

Using 3,5-bis(4-nitrophenoxy)benzoate (8) (25.6 g, 64.6 mmol) obtained in Example 4 and n-hexadecyl alcohol (17.3 g, 71.5 mmol), n-hexadecyl[3,5-bis(4-nitrophenoxy)]benzoate was obtained (32.4 g, yield: 81%) in the same manner as in Example 4.

Sources & evidence

ORD record: ord-2840ab729eff4eb0946f468265587741
Source dataset: uspto-grants-2004_05
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US06740371B1

Reaction notes

Loading…