HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-(Benzyloxy)-5-formylbenzoic acid → HCID 22716808, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-(Benzyloxy)-5-formylbenzoic acid | HCID 969870 | — |
| Reactant | 2,4-Difluorobenzyl 2-(2,4-difluorobenzyloxy)-5-formylbenzoate | HCID 22716817 | — |
| Product | HCID 22716808 | HCID 22716808 | — |
Reaction Steps
2-(2,4-Difluorobenzyloxy)-5-formylbenzoic acid was prepared from 2,4-difluorobenzyl 2-(2,4-difluorobenzyloxy)-5-formylbenzoate (1.2 g, 1 eq) using the same procedure as for 2-benzyloxy-5-formylbenzoic acid. The product was obtained as a white powder (746 mg, 89%). 1H NMR (CDCl3) δ9.97 (s, 1H, O═C—H), 5.37 (s, 2H, CH2Ar).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06740670B2 |
| Source dataset | uspto-grants-2004_05 |
| ORD ID | ord-1890d1b8896f4c0d8b3c55aff15e654f |
| Source note | uspto-grants-2004_05 |