HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dibenzylamine → N,N-dibenzyl-2-benzyloxy-4-formylbenzamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dibenzylamine | HCID 7656 | — |
| Reactant | N-phenyl-N-methyl-2-benzyloxy-5-formylbenzamide | HCID 22716821 | — |
| Reactant | 2-Benzyloxy-4-formylbenzoic acid | HCID 22716825 | — |
| Product | N,N-dibenzyl-2-benzyloxy-4-formylbenzamide | HCID 22716781 | — |
Reaction Steps
N,N-dibenzyl-2-benzyloxy-4-formylbenzamide was prepared from 2-benzyloxy-4-formylbenzoic acid (146 mg, 1 eq) and dibenzylamine (0.22 mL, 2 eq) using the same procedure as for N-phenyl-N-methyl-2-benzyloxy-5-formylbenzamide. The product was obtained as a brown oil (236 g, 95%). 1H NMR (CDCl3) δ9.96 (s, 1H, O═C—H), 5.24 (m, 3H, OCH2Ph and NCH2Ph), 4.33 (d, 1H, NCH2Ph), 4.11 (m, 2H, NCH2Ph).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06740670B2 |
| Source dataset | uspto-grants-2004_05 |
| ORD ID | ord-12f6a936adef4cbda6fb689ee7095368 |
| Source note | uspto-grants-2004_05 |