Cyclopentadiene → HCID 22717329, compound

Participants

Reaction Conditions

Reaction Steps

As in Example 1, 1,3-cyclopentadiene (1.00 g, 15.13 mmol), trichlorosilane (8.19 g, 60.47 mmol) and tetrabutylphosphonium chloride (0.44 g, 1.49 mmol) were added in a 25 mL stainless steel tube under nitrogen atmosphere. After sealing the cylinder with a cap, the reactor was maintained at 180° C. for 10 hours. The resulting mixture was distilled to yield 0.45 g (yield: 9%) of 2,4-bis(trichlorosilyl)-1-pentene.

Provenance & Evidence