HuagongsheHuagongshe Chemistry Print Report · For research reference only
Carbon Dioxide → HCID 20260927, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Carbon Dioxide | HCID 280 | — |
| Reactant | Toluene | HCID 1140 | — |
| Reactant | HCID 20260917 | HCID 20260917 | — |
| Reactant | Butyllithium | HCID 178418339 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 20260927 | HCID 20260927 | — |
Reaction Steps
Successive treatment of 3-bromo-6-(2-hydroxyethyl)-2-methylbenzo[b]thiophene with n-butyl lithium in ether followed by carbon dioxide according to the method of Example 11(ii) gave 6-(2-hydroxyethyl)-2-methylbenzo[b]thiophene-3-carboxylic acid, m.p. 166°-169° C. (from toluene).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04551468 |
| Source dataset | uspto-grants-1985_11 |
| ORD ID | ord-ac493e46467d43c8bd41be607922d7a8 |
| Source note | uspto-grants-1985_11 |