Pyridine → HCID 20261075, compound

HRID 1583452Notes

Reaction equation

HRID 1583452 reaction equation
[P:1]([O-:28])([O:24][CH2:25][CH2:26]Br)([O:3][CH2:4][CH2:5][O:6][CH2:7][CH2:8][O:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH3:23])=[O:2].[N:29]1[CH:34]=[CH:33][CH:32]=[CH:31][CH:30]=1>>[P:1]([O-:28])([O:24][CH2:25][CH2:26][N+:29]1[CH:34]=[CH:33][CH:32]=[CH:31][CH:30]=1)([O:3][CH2:4][CH2:5][O:6][CH2:7][CH2:8][O:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH3:23])=[O:2]

Participants

3

Reactant 2

HCID 1049PyridineHCID 20261088HCID 20261088, compound

Product 1

HCID 20261075HCID 20261075, compound

Procedure

2-[2-(Tetradecyloxy)ethoxy]ethyl 2-bromoethyl phosphate obtained in Example 26 is reacted with pyridine and a conventional purification procedure of the reaction mixture gives the title compound as colorless solid.

Workup

  1. customa conventional purification procedure of the reaction mixture

Sources & evidence

ORD record
ord-25623c3ee6bc43b68c3788c3066af7de
Source dataset
uspto-grants-1985_11
Patent number
US04551532

Reaction notes

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