HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethyl Sulfoxide → HCID 13557279, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethyl Sulfoxide | HCID 679 | — |
| Reactant | N-Hydroxyphthalimide | HCID 10665 | — |
| Reactant | Sodium Acetate | HCID 517045 | — |
| Reactant | HCID 54203470 | HCID 54203470 | — |
| Product | HCID 13557279 | HCID 13557279 | — |
Reaction Steps
This compound was prepared in the manner of Example 6, Step B, using 150.0 grams (0.588 mole) of ethyl 4-bromo-2-methyl-2-methylthiobutanoate, 95.9 grams (0.588 mole) of N-hydroxyphthalimide and 53.0 grams (0.647 mole) of sodium acetate in 1000 ml of dimethyl sulfoxide. The yield of ethyl 1-methyl-2-methylthio-4-(phthalimidooxy)butanoate was 93.0 grams as an oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04552585 |
| Source dataset | uspto-grants-1985_11 |
| ORD ID | ord-8dbe74b130ce4627ab57bd36c795b4c6 |
| Source note | uspto-grants-1985_11 |