HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrazine hydrate (1:1) → HCID 13557284, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrazine hydrate (1:1) | HCID 24654 | — |
| Reactant | HCID 20258613 | HCID 20258613 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 13557284 | HCID 13557284 | 21.4% |
Reaction Steps
This reaction was run in the same manner as Example 6, Part B, using 52.5 grams (0.169 mole) of methyl 1-(phthalimidooxymethyl)benzoate and 17.0 grams (0.34 mole) of hydrazine hydrate in 800 ml of methanol to give 5.4 grams of 1H-2,3-benzoxazin-4(3H)-one; m.p. 123°-125° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04552585 |
| Source dataset | uspto-grants-1985_11 |
| ORD ID | ord-e964cb2eab3e4888b4b40492beed1e0d |
| Source note | uspto-grants-1985_11 |