HuagongsheHuagongshe Chemistry Print Report · For research reference only
S-sec-butyl ethylphosphonotrithioic acid → 2-Butanethiol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | S-sec-butyl ethylphosphonotrithioic acid | HCID 13564051 | — |
| Solvent | Triethylamine | HCID 8471 | — |
| Product | 2-Butanethiol | HCID 10560 | — |
| Product | Phosphenodithioic ethane | HCID 16131073 | — |
Reaction Steps
(a.) Following the procedure as shown in Example 1, step (a), 14.67 g (94%) of the triethylamine salt of S-sec-butyl ethylphosphonotrithioic acid was obtained from 6.0 g (0.0242 mole) of ethylthionophosphine sulfide, 5.80 ml (4.58 g, 0.0508 mole) of sec-butyl mercaptan, and 7.1 ml (5.14 g, 0.0508 mole) of triethylamine.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04552870 |
| Source dataset | uspto-grants-1985_11 |
| ORD ID | ord-8eb01f63212d42a8beb3d243bfdfc538 |
| Source note | uspto-grants-1985_11 |