huagongshe.com
HRID1583715

反应详情

EQUATION

反应方程式

HRID 1583715 的结构方程式

REACTANTS

反应物

3
结构：OB(O)O
HCID7628

Boric acid (H3BO3)

H3BO3

结构：O=C(O)[C@H](O)[C@@H](O)[C@H](O)[C@H](O)CO
HCID10690

Gluconic acid

C6H12O7

结构：[Ca+2].[O-2]
HCID6850728

Calcium oxide

CaO

PRODUCTS

生成物

1
结构：O=C([O-])C(O)C(O)C1OB(O)OC1CO.O=C([O-])C(O)C(O)C1OB(O)OC1CO.[Ca+2]
HCID21969

Calcium bis{2,3-dihydroxy-3-[2-hydroxy-5-(hydroxymethyl)-1,3,2-dioxaborolan-4-yl]propanoate}

C12H20B2CaO16

收率 40%

AUXILIARIES

试剂、催化剂与溶剂

1
结构：O
溶剂HCID962

Water

H2O

2 次

PROCEDURE

实验过程

28 grams of calcium oxide were added to water to form a thick slurry. This slurry was slowly added with stirring to 392 grams of a 50% aqueous solution of technical grade gluconic acid. After all of the slurry was added the resultant mixture was cooled and 61.8 grams of technical grade boric acid added. The mixture was stirred until a dark brown solution was obtained and then adjusted by water addition to provide a 40% solids solution.

WORKUP

后处理

  1. customto form a thick slurry
  2. additionThis slurry was slowly added
  3. temperaturewas cooled
  4. customwas obtained