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Alanine ethylamide → 1-[(Benzyloxy)carbonyl]-L-prolyl-L-alanyl-N-ethyl-L-alaninamide
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Alanine ethylamide | HCID 7128993 | — |
| 反応物 | HCID 13749962 | HCID 13749962 | — |
| 反応物 | HCID 13750026 | HCID 13750026 | — |
| 溶媒 | Dimethylformamide | HCID 6228 | — |
| 生成物 | 1-[(Benzyloxy)carbonyl]-L-prolyl-L-alanyl-N-ethyl-L-alaninamide | HCID 13750028 | 49% |
反応手順
This product was prepared by a process analogous to that employed in preparing the corresponding benzyloxycarbonylalanylalanyl alanine ethylamide described in Example 1 from benzyloxycarbonylprolyl alanine hydrazide and alanine ethylamide in a 49% yield with a melting point of 219 to 220 degrees C. [α]D20 -36.2 degrees (c 0.3; dimethylformamide).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04554100 |
| 出典データセット | uspto-grants-1985_11 |
| ORD ID | ord-a9333cbb6a7e4f47ae5bee1354fecb4c |
| 出典メモ | uspto-grants-1985_11 |