HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 54351986, compound → 6-(4-Chlorophenyl)hexanoic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 54351986 | HCID 54351986 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | 6-(4-Chlorophenyl)hexanoic acid | HCID 13503441 | — |
Reaction Steps
A mixture of 49.3 g (0.219 mole) of 6-(p-chlorophenyl)hex-5-enoic acid, 3.0 g of 10% Pd/C, and 300 ml of ethyl acetate was hydrogenated at 45 psi and room temperature for 20 hours. The catalyst was removed by filtration through a Celite pad, and the filtrate concentrated to give 21.3 g (43%) of V as an oil, which was used without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04554276 |
| Source dataset | uspto-grants-1985_11 |
| ORD ID | ord-5f1d7963ee954557a37b05ff68d7d817 |
| Source note | uspto-grants-1985_11 |