7-Hydrazino-2,3dihydro-2-methylbenzofuran → HCID 13535833, compound

HRID 1583755Notes

Reaction equation

HRID 1583755 reaction equation
[NH:1]([C:3]1[C:11]2[O:10][C:9]([CH3:13])([CH3:12])[CH2:8][C:7]=2[C:6]([CH3:14])=[CH:5][CH:4]=1)[NH2:2].ClC(N(C1C2OC(C)CC=2C=CC=1)N[C:20]([N:22]([O:24][CH3:25])[CH3:23])=[O:21])=O.N(C1C2[O:45][CH:44](C)CC=2C=CC=1)N>>[CH3:13][C:9]1([CH3:12])[CH2:8][C:7]2[C:6]([CH3:14])=[CH:5][CH:4]=[C:3]([N:1]3[N:2]=[C:20]([N:22]([O:24][CH3:25])[CH3:23])[O:21][C:44]3=[O:45])[C:11]=2[O:10]1

Participants

4

Reactant 3

HCID 135358277-Hydrazino-2,3dihydro-2-methylbenzofuranHCID 13535829HCID 13535829, compoundHCID 13535832(2,3-Dihydro-2,2,4-trimethyl-7-benzofuranyl)hydrazine

Product 1

HCID 13535833HCID 13535833, compound

Procedure

3 was prepared, as an amber syrup, by treating 7-hydrazino-2,3-dihydro-2,2,4-trimethylbenzofuran (prepared by the method described in U.S. Pat. No. 4,406,910) according to the procedures described in Example 1 for preparing 1F from 1D.

Workup

  1. custom3 was prepared, as an amber syrup
  2. customprepared by the method

Sources & evidence

ORD record
ord-9204112cd66d4dc1b52b03905c5cbf11
Source dataset
uspto-grants-1985_11
Patent number
US04554283

Reaction notes

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