Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Nitromethane → 2,4-Dimethoxy-1-(2-nitroethenyl)benzene
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Nitromethane | HCID 6375 | — |
| 반응물 | 2,4-Dimethoxybenzaldehyde | HCID 69175 | — |
| 반응물 | Ammonium Acetate | HCID 517165 | — |
| 용매 | Acetic Acid | HCID 176 | — |
| 생성물 | 2,4-Dimethoxy-1-(2-nitroethenyl)benzene | HCID 275405 | — |
반응 단계
A mixture of 100 g of 2,4-dimethoxybenzaldehyde, 102 ml of nitromethane, 46.4 g of ammonium acetate and 500 ml of glacial acetic acid was heated at reflux for 2 hours and quenched in 700 ml of water. The crude precipitate was recrystallized from ethanol to give 105.57 g of 1-(2,4-dimethoxyphenyl)-2-nitroethylene as a yellow solid.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04554284 |
| 출처 데이터셋 | uspto-grants-1985_11 |
| ORD ID | ord-24d5ee03ef2b425297f1043a5e859639 |
| 출처 메모 | uspto-grants-1985_11 |