HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Methoxide → HCID 54566435, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Methoxide | HCID 10942334 | — |
| Reactant | HCID 54329042 | HCID 54329042 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 54566435 | HCID 54566435 | — |
Reaction Steps
Compound 21 is deacetylated with sodium methoxide in methanol to give 22 in near quantitative yield: [α]D27 +354° (C 1.0, chloroform); MS:m/e 296 (M.+), 278 (M.+ --H2O), 147 (M.+ --SCH2CH=CHC6H5).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04554349 |
| Source dataset | uspto-grants-1985_11 |
| ORD ID | ord-07745daad9b9412a8c6e3aa695dcbb4b |
| Source note | uspto-grants-1985_11 |