HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sulfuric Acid → 2-Amino-6-(3,4-dimethylphenyl)-6-methylheptane
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sulfuric Acid | HCID 1118 | — |
| Reactant | O-Xylene | HCID 7237 | — |
| Reactant | Heptaminol Hydrochloride | HCID 10969 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | 2-Amino-6-(3,4-dimethylphenyl)-6-methylheptane | HCID 20258552 | — |
Reaction Steps
21.2 Parts of o-xylene, 128 parts of 98% w/w sulphuric acid, 24 parts of methanol, and 36.3 parts of heptaminol hydrochloride were stirred at room temperature for 3 days. The work up was carried out as described in Example 2 and gave on distillation 36.2 parts of 2-amino-6-(3,4-dimethylphenyl)-6-methylheptane b16 164°-8° with the following percentage composition by weight.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04554379 |
| Source dataset | uspto-grants-1985_11 |
| ORD ID | ord-2842386169e142f2a1a2f095751de616 |
| Source note | uspto-grants-1985_11 |