Toluene → HCID 178506801, compound

HRID 1584028Notes

Reaction equation

HRID 1584028 reaction equation
C([Li:5])CCC.[C:6]1([C:12]([C:14]2[CH:19]=[CH:18][CH:17]=[CH:16][CH:15]=2)=[CH2:13])[CH:11]=[CH:10][CH:9]=[CH:8][CH:7]=1.[C:20]1(C)C=C[CH:23]=[CH:22][CH:21]=1>>[C:6]1([C:12]([Li:5])([C:14]2[CH:15]=[CH:16][CH:17]=[CH:18][CH:19]=2)[CH2:13][CH2:20][CH2:21][CH2:22][CH3:23])[CH:11]=[CH:10][CH:9]=[CH:8][CH:7]=1

Participants

4

Reactant 3

HCID 1140TolueneHCID 107401,1-DiphenylethyleneHCID 178418339Butyllithium

Product 1

HCID 178506801HCID 178506801, compound

Procedure

1,1-Diphenylhexyllithium was prepared by reacting n-butyllithium with 1,1-diphenylethylene in toluene at 40° C. for 72 h.

Workup

  1. customat 40° C.
  2. customfor 72 h.

Sources & evidence

ORD record
ord-6f42b8bf8f5e4fe9a35220a47813e6ef
Source dataset
uspto-grants-1985_11
Patent number
US04555574

Reaction notes

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