HCID 21224553, compound → HCID 21224543, compound

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Reaction Steps

A solution of 1-t-butylmethylaminocarbonylmethyl-4-methyl-5-azidomethylimidazole (400 mg) and 10% Pd/C (400 mg) in ethyl acetate (60 ml) was hydrogenated at atmospheric pressure for 4 h. The solution was filtered through Celite and the solvents removed in vacuo to give the title compound. 1H NMR (CDCl3) d 0.80 (s, 9 H), 1.61 (br s, 2 H), 2.23 (s, 3 H), 2.99 (d, J=6.1 Hz, 2 H), 3.86 (s, 2 H), 4.63 (s, 2 H), 7.50 (s, 1 H).

Provenance & Evidence