HCID 21224560, compound → HCID 21224503, compound

Participants

Reaction Steps

A solution of 1-t-butylaminocarbonylmethyl-4-methyl-5-azidomethylimidazole (1.27 g, 5.4 mmol) and 10% Pd/C (700 mg) in ethyl acetate (100 ml) was hydrogenated at atmospheric pressure for 5 h. The catalyst was removed by filtration through Celite and the solvents removed in vacuo to give the title compound. 1H NMR (CDCl3) d 1.27 (s, 9 H), 2.23 (s, 3 H), 3.83 (s, 2 H), 4.50 (s, 2 H), 7.08 (br s, 1 H), 7.46 (s, 1 H).

Provenance & Evidence