HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,4-Oxazolidinedione → 5-[3-[3-Methoxy-4-(5-methyl-2-phenyl-4-oxazolylmethoxy)phenyl]propyl]-2,4-oxazolidinedione
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,4-Oxazolidinedione | HCID 97389 | — |
| Reactant | 3-Methoxy-4-(5-methyl-2-phenyl-4-oxazolylmethoxy)cinnamaldehyde | HCID 53822879 | — |
| Product | 5-[3-[3-Methoxy-4-(5-methyl-2-phenyl-4-oxazolylmethoxy)phenyl]propyl]-2,4-oxazolidinedione | HCID 11026487 | — |
Reaction Steps
In substantially the same manner as in Working Example 11, 3-methoxy-4-(5-methyl-2-phenyl-4-oxazolyl-methoxy)cinnamaldehyde was condensed with 2,4-oxazolidinedione. The condensate was subjected to catalytic hydrogenation to yield 5-[3-[3-methoxy-4-(5-methyl-2-phenyl-4-oxazolylmethoxy)phenyl]propyl]-2,4-oxazolidinedione, which was recrystallized from ethyl acetate-hexane to give colorless prisms, m.p.161-162° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05932601 |
| Source dataset | uspto-grants-1999_08 |
| ORD ID | ord-6848d1b153d74a63a148abe6615f3cba |
| Source note | uspto-grants-1999_08 |