HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diisobutylaluminumhydride → HCID 21224432, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diisobutylaluminumhydride | HCID 21225700 | — |
| Reactant | HCID 54560603 | HCID 54560603 | — |
| Product | HCID 21224432 | HCID 21224432 | — |
Reaction Steps
In substantially the same manner as in Reference Example 24, methyl 4-methoxy-3-(5-methyl-2-phenyl-4-oxazolylmethoxy)cinnamate was subjected to reduction with diisobutyl aluminum hydride to yield (E)-3-[4-methoxy-3-(5-methyl-2-phenyl-4-oxazolylmethoxy)phenyl]-2-propen-1-ol, which was recrystallized from ethyl acetate-ether to give pale yellow prisms, m.p.137-138° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05932601 |
| Source dataset | uspto-grants-1999_08 |
| ORD ID | ord-74fc28967bb14ca1a969b2f66e3f9311 |
| Source note | uspto-grants-1999_08 |