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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1584409Generated: November 1, 2026

HCID 53718425, compound → HCID 54213503, compound

https://huagongshe.com/reaction/1584409

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 53718425HCID 53718425—
CatalystPalladiumHCID 23938—
SolventEthanolHCID 702—
ProductHCID 54213503HCID 54213503—

Reaction Steps

(R)-2-(benzyloxycarbonylamino)-N-tert-butoxy-3-(4-phenoxyphenylsulfonyl)-propionamide (6.0 g) obtained from Example 17 was dissolved in ethanol (100 ml) and hydrogenated at 1 atmosphere in the presence of 10% palladium on carbon (6 g) for a period of 18 hours. The catalyst was filtered off and the solvent removed from the filtrate under reduced pressure to give (R)-2-amino-N-tert-butoxy-3-(4-phenoxyphenylsulfonyl)-propionamide as a glass.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05932595
Source datasetuspto-grants-1999_08
ORD IDord-4b114916e5dd48e5a2303282668e0d6a
Source noteuspto-grants-1999_08