HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 53718425, compound → HCID 54213503, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 53718425 | HCID 53718425 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 54213503 | HCID 54213503 | — |
Reaction Steps
(R)-2-(benzyloxycarbonylamino)-N-tert-butoxy-3-(4-phenoxyphenylsulfonyl)-propionamide (6.0 g) obtained from Example 17 was dissolved in ethanol (100 ml) and hydrogenated at 1 atmosphere in the presence of 10% palladium on carbon (6 g) for a period of 18 hours. The catalyst was filtered off and the solvent removed from the filtrate under reduced pressure to give (R)-2-amino-N-tert-butoxy-3-(4-phenoxyphenylsulfonyl)-propionamide as a glass.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05932595 |
| Source dataset | uspto-grants-1999_08 |
| ORD ID | ord-4b114916e5dd48e5a2303282668e0d6a |
| Source note | uspto-grants-1999_08 |