(4-Chlorophenyl)hydrazine → HCID 21220538, compound

HRID 1584729Notes

Reaction equation

HRID 1584729 reaction equation
O=[C:2]1[CH:11]([CH2:12][C:13]([O:15]C)=O)[CH2:10][CH2:9][C:8]2[N:7]=[CH:6][CH:5]=[CH:4][C:3]1=2.N1C2CCCC(=O)C=2C=CC=1.[Cl:28][C:29]1[CH:34]=[CH:33][C:32]([NH:35][NH2:36])=[CH:31][CH:30]=1>>[Cl:28][C:29]1[CH:34]=[CH:33][C:32]([N:35]2[C:13](=[O:15])[CH2:12][CH:11]3[C:2]([C:3]4[CH:4]=[CH:5][CH:6]=[N:7][C:8]=4[CH2:9][CH2:10]3)=[N:36]2)=[CH:31][CH:30]=1

Participants

4

Reactant 3

HCID 70624(4-Chlorophenyl)hydrazineHCID 30168115(6H)-Quinolinone, 7,8-dihydro-HCID 54422203HCID 54422203, compound

Product 1

HCID 21220538HCID 21220538, compound

Procedure

Prepared according to the method described in Example 1 from methyl 5,6,7,8-tetrahydro-5-oxoquinoline-6-acetate (prepared from 7,8-dihydroquinoline-5(6H)-one (J. Med. Chem. (1991)34, 2736) according to the method of Wu et al supra) and 4-chlorophenylhydrazine.

Workup

  1. customPrepared

Sources & evidence

ORD record
ord-564c2d6f181e4e448af08bc434a5a045
Source dataset
uspto-grants-1999_08
Patent number
US05935956

Reaction notes

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