(4-Chlorophenyl)hydrazine → HCID 21220528, compound

HRID 1584730Notes

Reaction equation

HRID 1584730 reaction equation
O=[C:2]1[C:11]2[CH2:10][NH:9][CH2:8][CH2:7][C:6]=2[CH:5]=[CH:4][CH:3]1[CH2:12][C:13]([O-:15])=O.N1C2C(=O)CCCC=2C=CC=1.[Cl:27][C:28]1[CH:33]=[CH:32][C:31]([NH:34][NH2:35])=[CH:30][CH:29]=1>>[Cl:27][C:28]1[CH:33]=[CH:32][C:31]([N:34]2[C:13](=[O:15])[CH2:12][CH:3]3[C:2]([C:11]4[CH:10]=[N:9][CH:8]=[CH:7][C:6]=4[CH2:5][CH2:4]3)=[N:35]2)=[CH:30][CH:29]=1

Participants

4

Reactant 3

HCID 70624(4-Chlorophenyl)hydrazineHCID 117447776,7-Dihydro-5H-quinoline-8-oneHCID 86754385HCID 86754385, compound

Product 1

HCID 21220528HCID 21220528, compound

Procedure

Prepared according to the method described in Example 1 from methyl 5,6,7,8, -tetrahydro-8-oxoisoquinoline-7-acetate (prepared from 5,6-dihydroquinoline-8(7H)-one (Boyd et al, J. Chem. Soc., Perkin Trans. I (1992)31) according to the method of Wu et al supra) and 4-chlorophenylhydrazine.

Workup

  1. customPrepared

Sources & evidence

ORD record
ord-f4922f114e7f424ba077fad3bdec3d11
Source dataset
uspto-grants-1999_08
Patent number
US05935956

Reaction notes

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