(4-Chlorophenyl)hydrazine → HCID 21220531, compound

HRID 1584731Notes

Reaction equation

HRID 1584731 reaction equation
O=[C:2]1[C:11]2[N:10]=[CH:9][CH:8]=[CH:7][C:6]=2[CH2:5][CH2:4][CH:3]1[CH2:12][C:13]([O:15]C)=O.N1C2C(=O)CCCC=2C=CC=1.[Cl:28][C:29]1[CH:34]=[CH:33][C:32]([NH:35][NH2:36])=[CH:31][CH:30]=1>>[Cl:28][C:29]1[CH:34]=[CH:33][C:32]([N:35]2[C:13](=[O:15])[CH2:12][CH:3]3[C:2]([C:11]4[N:10]=[CH:9][CH:8]=[CH:7][C:6]=4[CH2:5][CH2:4]3)=[N:36]2)=[CH:31][CH:30]=1

Participants

4

Reactant 3

HCID 70624(4-Chlorophenyl)hydrazineHCID 117447776,7-Dihydro-5H-quinoline-8-oneHCID 53799449HCID 53799449, compound

Product 1

HCID 21220531HCID 21220531, compound

Procedure

Prepared according to the method described in Example 1 from methyl 5,6,7,8-tetrahydro-8-oxoquinoline-7-acetate (prepared from 6,7-dihydroquinoline-8(5H)-one according to the method of Wu et al supra) and 4-chlorophenylhydrazine.

Workup

  1. customPrepared

Sources & evidence

ORD record
ord-93270e263a5343ec9444ea472466ca4f
Source dataset
uspto-grants-1999_08
Patent number
US05935956

Reaction notes

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