HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 21220912, compound → 5-Bromo-1-benzofuran-7-carbaldehyde
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 21220912 | HCID 21220912 | — |
| Catalyst | HCID 178418406 | HCID 178418406 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | 5-Bromo-1-benzofuran-7-carbaldehyde | HCID 21220840 | 95.3% |
Reaction Steps
A solution of (5-bromo-benzofuran-7-yl)-methanol (327 mg) in 1,4-dioxan (20 ml ) was treated with manganese dioxide (371 mg) and heated at reflux for 2 h. The reaction mixture was filtered, the cake was washed with chloroform (30 ml) and the combined filtrates were evaporated in vacuo to give the title compound as an orange solid (309 mg).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05935972 |
| Source dataset | uspto-grants-1999_08 |
| ORD ID | ord-b71084edc9be49c39e9a63a34c646de4 |
| Source note | uspto-grants-1999_08 |