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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1584772Generated: October 31, 2026

HCID 21220912, compound → 5-Bromo-1-benzofuran-7-carbaldehyde

https://huagongshe.com/reaction/1584772

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 21220912HCID 21220912—
CatalystHCID 178418406HCID 178418406—
Solvent1,4-DioxaneHCID 31275—
Product5-Bromo-1-benzofuran-7-carbaldehydeHCID 2122084095.3%

Reaction Steps

A solution of (5-bromo-benzofuran-7-yl)-methanol (327 mg) in 1,4-dioxan (20 ml ) was treated with manganese dioxide (371 mg) and heated at reflux for 2 h. The reaction mixture was filtered, the cake was washed with chloroform (30 ml) and the combined filtrates were evaporated in vacuo to give the title compound as an orange solid (309 mg).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05935972
Source datasetuspto-grants-1999_08
ORD IDord-b71084edc9be49c39e9a63a34c646de4
Source noteuspto-grants-1999_08