Sodium Hydroxide → HCID 15428568, compound

Participants

Reaction Steps

A solution of 4-(7-[1,3]dioxan-2-yl-benzofuran-5-yl)-2H-[1,2,3]triazole (80 mg) in hydrochloric acid (2M; 10 ml) and tetrahydrofuran was heated at reflux for 0.5 h. The cooled reaction mixture was treated with sodium hydroxide (25 ml; 2M) and extracted with ethyl acetate (3×50 ml). The combined organic extracts were dried, and evaporated in vacuo to give the title compound as a yellow/orange solid (60 mg).

Provenance & Evidence