HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrazine → HCID 21220622, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrazine | HCID 9321 | — |
| Reactant | HCID 21220675 | HCID 21220675 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 21220622 | HCID 21220622 | 99% |
Reaction Steps
The title compound was prepared as described in Example 18, but employing a solution of ethyl 2-chloro-4-benzylpyrimidine-5-carboxylate (0.34 g, 1.2 mmol) and hydrazine (0.2 g, 6.1 mmol) in THF resulting in a 99% yield (0.33 g, oil); GC/MS, 272(M+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05935966 |
| Source dataset | uspto-grants-1999_08 |
| ORD ID | ord-645bf936d73149f1b396bfd50688e497 |
| Source note | uspto-grants-1999_08 |