HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Furoyl chloride → N-(N,N-Diethyl-1,2,3,4-tetrahydro-2-aminodibenzofur-8-yl)-3-furamide hydrochloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Furoyl chloride | HCID 2776123 | — |
| Reactant | 8-Amino-1,2,3,4-tetrahydro-2-diethylaminodibenzofuran | HCID 21221558 | — |
| Product | N-(N,N-Diethyl-1,2,3,4-tetrahydro-2-aminodibenzofur-8-yl)-3-furamide hydrochloride | HCID 21221578 | 69.4% |
Reaction Steps
Beginning with 0.100 gm (0.30 mMol) 8-amino-1,2,3,4-tetrahydro-2-diethylaminodibenzofuran and 0.052 gm (0.40 mMol) furan-3-carbonyl chloride, 0.081 gm (69%) of the title compound were recovered as an off-white solid by the procedure described in Example 17.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05935992 |
| Source dataset | uspto-grants-1999_08 |
| ORD ID | ord-4d8761828f6c42ba819d398217eddbfa |
| Source note | uspto-grants-1999_08 |