Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | HCID 11011640 | HCID 11011640 | — |
| Reactant | HCID 15428727 | HCID 15428727 | — |
| Product | 3-Phenylindole | HCID 96502 | 207.5% |
Reaction Steps
By following the procedure of Example 1 substantially faithfully while using N-tosyl-D-prolyl chloride in the place of benzoyl chloride and changing the reaction temperature during the course of cooling to -40° C., 3.88 g of 3-phenyl-1-(N-tosyl-D-prolyl)indole (48.2%) having a melting point of 148-149° C. was obtained from 3.50 g of 3-phenylindole.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US05936098 |
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| Source dataset | uspto-grants-1999_08 |
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| ORD ID | ord-81d4534ea3bc42b5a5dff312efc2db15 |
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| Source note | uspto-grants-1999_08 |
|---|
