HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1585286Generated: October 25, 2026
Diethyl Ether → 2-[5-(2,6-Dimethoxyphenyl)-1-[4-[N-methyl-N-(3-dimethylaminopropyl)carbamoyl]-2-isopropylphenyl]-3-pyrazolylcarbonylamino]-2-adamantanecarboxylic acid benzenesulphonate
https://huagongshe.com/reaction/1585286
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Diethyl Ether | HCID 3283 | — |
| Reactant | Benzenesulfonic Acid | HCID 7371 | — |
| Reactant | SR142948A | HCID 5311451 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | 2-[5-(2,6-Dimethoxyphenyl)-1-[4-[N-methyl-N-(3-dimethylaminopropyl)carbamoyl]-2-isopropylphenyl]-3-pyrazolylcarbonylamino]-2-adamantanecarboxylic acid benzenesulphonate | HCID 86754283 | 9.8% |
Reaction Steps
A mixture of 0.5 g of the compound obtained in EXAMPLE 1' and 0.16 g of benzenesulphonic acid in 5 ml of MeOH is poured into 75 ml of ether cooled to 5° C., and the precipitate formed is drained. 0.06 g of the expected product is obtained, m.p.=170° C. (dec.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US05936123 |
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| Source dataset | uspto-grants-1999_08 |
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| ORD ID | ord-076f15100bd444519e7dd5acc289824c |
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| Source note | uspto-grants-1999_08 |
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