関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | SR142948A | HCID 5311451 | — |
| 反応物 | HCID 178418600 | HCID 178418600 | — |
| 溶媒 | Methanol | HCID 887 | — |
| 生成物 | HCID 178491337 | HCID 178491337 | 43.9% |
反応手順
0.1 g of the compound obtained in EXAMPLE 1' and 0.03 g of (S)-(+)-arginine are dissolved in the heated state in 4 ml of MeOH, and this solution is concentrated to 1 ml and poured into 10 ml of ether cooled to 5° C. 0.055 g of the expected product is obtained after draining and drying over P2O5, m.p.=176° C.(dec.).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 特許番号 | US05936123 |
|---|
| 出典データセット | uspto-grants-1999_08 |
|---|
| ORD ID | ord-f7cfe8d94b1144d4aae668af2c4dc686 |
|---|
| 出典メモ | uspto-grants-1999_08 |
|---|
